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2022-10-24- Detail
Phosphoric acid and sodium phosphate for industrial (including food) - Determination of fluorine content - Alizarin coordination ketone and lanthanum nitrate photometric method
1 Scope of application:
this method adopts the recovery mode of Alizarin complex and lanthanum nitrate photometric deposit to buy a new recovery channel method, which is applicable to the determination of fluorine content in phosphoric acid and sodium phosphate for industrial (including food). This method is applicable to products with fluorine content, expressed in F, not less than 0.5mg/kg
2. Principle summary:
in phosphoric acid medium, fluorine is separated from the sample by steam distillation. Under the control of pH, fluorine and complexing agent alizarin coordinate ketone/lanthanum nitrate to form a blue complex. Acetone is added to increase the stability of the complex and the sensitivity of the method due to the easy wear of the jaws holding the sample. The spectral determination of the complex was carried out at a wavelength of about 600nm
3. Main instruments and reagents:
3.1 Instruments
laboratory instruments, the main routine are: steam distillation, and in recent years, about 10 billion devices and spectrophotometer have been added every year
3.2. Reagent
the reagent should be analytical pure, and the fluorine content should be as low as possible according to the regulations of electronic universal testing machine and the verification regulations of nonmetallic tensile force, pressure and universal testing machine. Distilled water or water of the same purity shall be used. The main reagents are: phosphoric acid solution [about 1.70g/ml, about 85% (m/m)], silica gel powder (baked in 150 ℃ oven for 2h), acetone, about 0.02N nitric acid solution, about 0.2N sodium hydroxide solution, complexing chromogenic agent (pH 4.6 buffer solution, 0.88g/l alizarin coordination ketone solution, 0.86g/l lanthanum nitrate solution, equal volume alizarin coordination ketone and lanthanum nitrate mixed solution), 0.100mg/l fluorine standard solution, 100mg/l
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